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LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng. Synthesis of hairpin-polyamides containing β-alanine[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(3): 217-219,231.
Citation: LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng. Synthesis of hairpin-polyamides containing β-alanine[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(3): 217-219,231.

Synthesis of hairpin-polyamides containing β-alanine

  • Received Date: 2009-11-04
  • Rev Recd Date: 2010-01-22
  • Objective To develop a new method and strategy for the synthesis of hairpin-polyamides containingβ-alanine. Methods The hairpin-polyamides were synthesized by the HOBT/DCC coupling reaction in good yields through the optimization of hydrogenation of nitro group and the 2+2 fragment coupling strategy. Results A hairpin-polyamide NO2ImPyβImPyγImPyβPyPyβCOOC2H2 was synthesized successfully with good yield. Conclusion The hairpin-polyamides containing β-alanine in the molecular can be easily and efficiently synthesized through the optimization of reaction temperature,solvent and fragment coupling strategy.
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通讯作者: 陈斌, [email protected]
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    沈阳化工大学材料科学与工程学院 沈阳 110142

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Synthesis of hairpin-polyamides containing β-alanine

Abstract: Objective To develop a new method and strategy for the synthesis of hairpin-polyamides containingβ-alanine. Methods The hairpin-polyamides were synthesized by the HOBT/DCC coupling reaction in good yields through the optimization of hydrogenation of nitro group and the 2+2 fragment coupling strategy. Results A hairpin-polyamide NO2ImPyβImPyγImPyβPyPyβCOOC2H2 was synthesized successfully with good yield. Conclusion The hairpin-polyamides containing β-alanine in the molecular can be easily and efficiently synthesized through the optimization of reaction temperature,solvent and fragment coupling strategy.

LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng. Synthesis of hairpin-polyamides containing β-alanine[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(3): 217-219,231.
Citation: LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng, LI Peng. Synthesis of hairpin-polyamides containing β-alanine[J]. Journal of Pharmaceutical Practice and Service, 2010, 28(3): 217-219,231.

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