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Volume 34 Issue 2
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2016  >  34(2): 167-170

ZHAO Xin, WANG Shenge, Xu Zhijun, CHEN Mingming. Study on quality standard of Weinaxin granular[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(2): 167-170. doi: 10.3969/j.issn.1006-0111.2016.02.017
Citation: ZHAO Xin, WANG Shenge, Xu Zhijun, CHEN Mingming. Study on quality standard of Weinaxin granular[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(2): 167-170. doi: 10.3969/j.issn.1006-0111.2016.02.017
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Study on quality standard of Weinaxin granular

doi: 10.3969/j.issn.1006-0111.2016.02.017
  • 1.

    Institute for Drug and Instrument Control of Shenyang Military Region, Shenyang 110026, China

  • 2.

    General Hospital of Shenyang Military Region, Shenyang 110016

  • 3.

    Public Computer Teaching and Research Center, Jilin University, Changchun 130062, China

  • Received Date: 2014-12-17
  • Rev Recd Date: 2015-08-31
  • Objective To establish a quality standard of Weinaxin granular. Methods Pinelliae Rhizoma,Poria,Glycyrrhizae, Radix Angelicae,Aurantii Fructus were identified by TLC,and the assay of Narigin in Aurantii Fructus was performed by reverse phase HPLC. Results Pinelliae Rhizoma,Poria,Glycyrrhizae,Radix Angelicae,Aurantii Fructus can be identified by TLC. The HPLC method for Narigin shows a baseline separation with a linear calibration curve in the range of 0.0844~0.2954μg(r=0.9993). The average recovery of the method was 98.74%.The RSD was 1.20%(n=6). Conclusion This method was reliable and accurate,can be used for the quality control of this product.
  • [1] 李雪婷,王沛, 崔晓立.紫外分光光度法测定痛风宁微丸中柚皮苷的含量[J].中国卫生工程学,2011,3:38-39.
    [2] 李慧.高效液相色谱法测定橘红痰咳液中柚皮苷的含量[J].药品检验,2012,9(5):110-111.
    [3] 邓秋丽,徐文升,李胜.RP-HPLC法测定祛瘀散结胶囊中柚皮苷的含量[J].中国医药指南,2010,8(30):13-14.
    [4] 国家药典委员会.中华人民共和国国药典2010年版一部[S].北京:中国医药科技出版社,2010:542-543.
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Study on quality standard of Weinaxin granular

doi: 10.3969/j.issn.1006-0111.2016.02.017
  • 1. Institute for Drug and Instrument Control of Shenyang Military Region, Shenyang 110026, China
  • 2. General Hospital of Shenyang Military Region, Shenyang 110016
  • 3. Public Computer Teaching and Research Center, Jilin University, Changchun 130062, China
  • Received Date: 2014-12-17
  • Rev Recd Date: 2015-08-31

Abstract: Objective To establish a quality standard of Weinaxin granular. Methods Pinelliae Rhizoma,Poria,Glycyrrhizae, Radix Angelicae,Aurantii Fructus were identified by TLC,and the assay of Narigin in Aurantii Fructus was performed by reverse phase HPLC. Results Pinelliae Rhizoma,Poria,Glycyrrhizae,Radix Angelicae,Aurantii Fructus can be identified by TLC. The HPLC method for Narigin shows a baseline separation with a linear calibration curve in the range of 0.0844~0.2954μg(r=0.9993). The average recovery of the method was 98.74%.The RSD was 1.20%(n=6). Conclusion This method was reliable and accurate,can be used for the quality control of this product.

ZHAO Xin, WANG Shenge, Xu Zhijun, CHEN Mingming. Study on quality standard of Weinaxin granular[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(2): 167-170. doi: 10.3969/j.issn.1006-0111.2016.02.017
Citation: ZHAO Xin, WANG Shenge, Xu Zhijun, CHEN Mingming. Study on quality standard of Weinaxin granular[J]. Journal of Pharmaceutical Practice and Service, 2016, 34(2): 167-170. doi: 10.3969/j.issn.1006-0111.2016.02.017
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