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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2015  >  33(6): 536-538

ZHANG Yan, WANG Qiang, REN Changshun, LANG Yiyong. Microemulsion TLC identification of Xinnaomaitong capsule[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(6): 536-538. doi: 10.3969/j.issn.1006-0111.2015.06.015
Citation: ZHANG Yan, WANG Qiang, REN Changshun, LANG Yiyong. Microemulsion TLC identification of Xinnaomaitong capsule[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(6): 536-538. doi: 10.3969/j.issn.1006-0111.2015.06.015
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Microemulsion TLC identification of Xinnaomaitong capsule

doi: 10.3969/j.issn.1006-0111.2015.06.015

  • No.202 Hospital of PLA, Shenyang 110003, China

  • Received Date: 2014-09-24
  • Rev Recd Date: 2015-06-08
  • Objective To investigate the application of microemulsion thin layer chromatography (TLC) for separation and identification of various active components in Xinnaomaitong capsule. Methods The all-grass of Bluecalyx japanese rabodosia, root of Pueraria lobata, root and rhizome of Salvia miltiorrhiza, rhizome of Ligusticum chuanxiong in Xinnaomaitong capsule were separated and identified simultaneously with the polyamide film as stationary phase and the microemulsion as mobile phases. Different factors, such as the sodium dodecyl sulfate (SDS), oil phase and water phase which effect on the separation of the components were evaluated. Results The all-grass of Bluecalyx japanese rabodosia, root of Pueraria lobata, root and rhizome of Salvia miltiorrhiza, rhizome of Ligusticum chuanxiong in Xinnaomaitong capsule were separated and identified simultaneously with mobile phase of microemulsion:formic acid:acetone (5:1:1). The constituent of microemulsion was SDS:butyl alcohol:n-Heptane:water = 6.7:15.8:2.5:75.0 (g/g). The spots were clear, the negative control was no interference, and it showed an ideal separation. Conclusion Microemulsion TLC is simple, accurate, and reproducible. It can identify a variety of active components in traditional Chinese medicine simultaneously.
  • [1] 康 纯,闻莉毓,丁仲伯,等.微乳薄层色谱用于黄连类药物分离鉴定的研究[J].中国中药杂志,2000,25(5): 262-265.
    [2] 陈培栋.微乳色谱应用研究进展[J].中国药房,2007,18(34): 2706.
    [3] 唐洪梅,闫 雪,李得堂.微乳TLC法分离鉴定肠激安方中多种有效成分[J].中国药房,2009,20(21): 1633-1635.
    [4] 陈 珏,齐炼文,李 萍.微乳及其在中药分析中的应用[J].药学进展,2013,37(9):441-448.
    [5] 郎轶咏,王 强,姜同英,等.三黄颗粒的微乳薄层色谱法鉴别[J].中国医院药学杂志,2009,29(6):469-472.
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Microemulsion TLC identification of Xinnaomaitong capsule

doi: 10.3969/j.issn.1006-0111.2015.06.015
  • No.202 Hospital of PLA, Shenyang 110003, China
  • Received Date: 2014-09-24
  • Rev Recd Date: 2015-06-08

Abstract: Objective To investigate the application of microemulsion thin layer chromatography (TLC) for separation and identification of various active components in Xinnaomaitong capsule. Methods The all-grass of Bluecalyx japanese rabodosia, root of Pueraria lobata, root and rhizome of Salvia miltiorrhiza, rhizome of Ligusticum chuanxiong in Xinnaomaitong capsule were separated and identified simultaneously with the polyamide film as stationary phase and the microemulsion as mobile phases. Different factors, such as the sodium dodecyl sulfate (SDS), oil phase and water phase which effect on the separation of the components were evaluated. Results The all-grass of Bluecalyx japanese rabodosia, root of Pueraria lobata, root and rhizome of Salvia miltiorrhiza, rhizome of Ligusticum chuanxiong in Xinnaomaitong capsule were separated and identified simultaneously with mobile phase of microemulsion:formic acid:acetone (5:1:1). The constituent of microemulsion was SDS:butyl alcohol:n-Heptane:water = 6.7:15.8:2.5:75.0 (g/g). The spots were clear, the negative control was no interference, and it showed an ideal separation. Conclusion Microemulsion TLC is simple, accurate, and reproducible. It can identify a variety of active components in traditional Chinese medicine simultaneously.

ZHANG Yan, WANG Qiang, REN Changshun, LANG Yiyong. Microemulsion TLC identification of Xinnaomaitong capsule[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(6): 536-538. doi: 10.3969/j.issn.1006-0111.2015.06.015
Citation: ZHANG Yan, WANG Qiang, REN Changshun, LANG Yiyong. Microemulsion TLC identification of Xinnaomaitong capsule[J]. Journal of Pharmaceutical Practice and Service, 2015, 33(6): 536-538. doi: 10.3969/j.issn.1006-0111.2015.06.015
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