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Volume 32 Issue 2
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2014  >  32(2): 92-95,106

LIN Shan, SU Juan, YE Ji, CAO Bangjing, ZHANG Weidong. Application progress in quantitative NMR in analysis of traditional Chinese medicine[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(2): 92-95,106. doi: 10.3969/j.issn.1006-0111.2014.02.004
Citation: LIN Shan, SU Juan, YE Ji, CAO Bangjing, ZHANG Weidong. Application progress in quantitative NMR in analysis of traditional Chinese medicine[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(2): 92-95,106. doi: 10.3969/j.issn.1006-0111.2014.02.004
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Application progress in quantitative NMR in analysis of traditional Chinese medicine

doi: 10.3969/j.issn.1006-0111.2014.02.004
  • 1.

    School of Pharmacy, Fujian Traditional Chinese Medicine University, Fuzhou 350108, China

  • 2.

    School of Pharmacy, Second Military Medical University, Shanghai 200433, China

  • 3.

    Department of Pharmacy, Jiangxi Traditional Chinese Medicine University, Nanchang 330004, China

  • Received Date: 2013-03-29
  • Rev Recd Date: 2013-09-07
  • Objective To review the principle of qNMR and applications progress in traditional Chinese medicine (TCM) analysis in recent ten years. Methods Literatures in recent ten years which concerning the application of qNMR technology in TCM analysis were reviewed. Results qNMR had high specificity and accuracy as a well-developed quantitative analysis method. Conclusion The qNMR had been used in many fields of TCM analysis, such as quality control, purity detection, quantification of active ingredients in vivo, and so on.
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    [2] Suter D, Mahesh TS. Spins as qubits:quantum information processing by nuclear magnetic resonance[J]. Chem Phys, 2008, 128(5):1-14.
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    [6] 陈玉兰, 陶凌晖, 侯 华,等. 核磁共振氢谱内标法测定盐酸小檗碱的含量[J]. 第三军医大学学报, 2009, 31(22):2217-2219.
    [7] Burton IW, Quilliam MA, Walter JA. Quantitative 1H-NMR with external standards:use in preparation of calibration solutions for algal toxins and other natural products[J]. Anal Chem, 2005, 77:3123-3131.
    [8] 李建发, 孙永跃, 蓝 丹,等. 1H-NMR定量分析葛根素含量研究[J]. 实验技术与管理, 2011, 28(12):36-39.
    [9] 李建发, 全志利, 蓝 丹. 核磁共振氢谱定量分析橙皮苷含量[J]. 实验技术与管理, 2012,31(6):18-21.
    [10] Jaki BU, Franzblau SG, Chadwick LR, et al. Purity activity relationships of natural products:the case of anti-TB active ursolic acid[J]. J Nat Prod, 2008, 71:1742-1748.
    [11] 薛松, 胡皆汉, 张卫. 氢谱在甾醇类化合物定量和纯度分析中的应用[J]. 分析化学学, 2003, 31(12):1493-1495.
    [12] Gang F, Meng Y, Zhang X, et al. Quality evaluation and species differentiation of rhizoma-coptidis by using proton nuclear magnetic resonance spectroscopy[J]. Anal Chim Acta, 2012, 747:76-83.
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    [14] Wen H, Kang S, Song Y, et al. Differentiation of cultivation sources of ganoderma lucidum-by NMR-based metabolomics approach[J]. Phytochem Anal, 2010, 21:73-79.
    [15] 江洪波, 姜建辉, 田仁君,等. 绵阳麦冬1H-NMR主成分分析暨质量控制研究[J]. 环球中医药, 2011, 4(3):190-192.
    [16] Li CY, Lu HJ, Lin CH, et al. A rapid and simple determination of protoberberine alkaloids in cortex phellodendri by 1H-NMR and its application for quality control of commercial traditional Chinese medicine prescriptions[J]. J Pharm Biomed Anal, 2006, 40:173-178.
    [17] Li CY, Lu HJ, Wu TS. Quantitative analysis of camptothecin derivatives in Nothapodytes foetida using 1H-NMR method[J]. Chem Pharm Bull, 2005,53(3):347-349.
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Application progress in quantitative NMR in analysis of traditional Chinese medicine

doi: 10.3969/j.issn.1006-0111.2014.02.004
  • 1. School of Pharmacy, Fujian Traditional Chinese Medicine University, Fuzhou 350108, China
  • 2. School of Pharmacy, Second Military Medical University, Shanghai 200433, China
  • 3. Department of Pharmacy, Jiangxi Traditional Chinese Medicine University, Nanchang 330004, China
  • Received Date: 2013-03-29
  • Rev Recd Date: 2013-09-07

Abstract: Objective To review the principle of qNMR and applications progress in traditional Chinese medicine (TCM) analysis in recent ten years. Methods Literatures in recent ten years which concerning the application of qNMR technology in TCM analysis were reviewed. Results qNMR had high specificity and accuracy as a well-developed quantitative analysis method. Conclusion The qNMR had been used in many fields of TCM analysis, such as quality control, purity detection, quantification of active ingredients in vivo, and so on.

LIN Shan, SU Juan, YE Ji, CAO Bangjing, ZHANG Weidong. Application progress in quantitative NMR in analysis of traditional Chinese medicine[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(2): 92-95,106. doi: 10.3969/j.issn.1006-0111.2014.02.004
Citation: LIN Shan, SU Juan, YE Ji, CAO Bangjing, ZHANG Weidong. Application progress in quantitative NMR in analysis of traditional Chinese medicine[J]. Journal of Pharmaceutical Practice and Service, 2014, 32(2): 92-95,106. doi: 10.3969/j.issn.1006-0111.2014.02.004
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