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Volume 30 Issue 2
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2012  >  30(2): 115-117

CHEN Jun, ZHOU Jin, HE Yun-xin, FENG Chun-hua, ZHANG Guo-qing. Analysis of volatile constituents in Caulis Sinomenii by GC-MS[J]. Journal of Pharmaceutical Practice and Service, 2012, 30(2): 115-117. doi: 10.3969/j.issn.1006-0111.2012.02.010
Citation: CHEN Jun, ZHOU Jin, HE Yun-xin, FENG Chun-hua, ZHANG Guo-qing. Analysis of volatile constituents in Caulis Sinomenii by GC-MS[J]. Journal of Pharmaceutical Practice and Service, 2012, 30(2): 115-117. doi: 10.3969/j.issn.1006-0111.2012.02.010
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Analysis of volatile constituents in Caulis Sinomenii by GC-MS

doi: 10.3969/j.issn.1006-0111.2012.02.010

  • Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China

  • Received Date: 2011-08-29
  • Rev Recd Date: 2011-12-28
  • Objective To establish the determination method for chemical constituents of the volatile oil in Sinornenium actum(Thunb.)Rehd.et Wils by gas chromatography-mass spectrometry(GC-MS). Method The volatile oil was extracted from Sinornenium actum(Thunb.)Rehd.et Wils by steam distillation.The constituents of volatile oil were identified by GC-MS technology,which were identified through database index. Results The results showed that after comparing of the gained mass spectrum with the standard, 63 kinds of chemical constituents in all were identified, the major constituents were the fatty acids, sterols, alkenes and a few kind of aldehyde. The most contents were octadecylic acid and hexadecanoic acid, whose relative percentages were 33.78% and 23.23% respectively. Conclusion The experiment improved the basic components study on Caulis Sinomenii, which could provide more reference quality control of Caulis Sinomenii.
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    [5] 任 洁,薛兴亚,章飞芳,等.气相色谱-质谱联用分析青风藤挥发油中化学成分[J].世界科学技术-中医药现代化,2006,8(3):21.
    [6] 江苏新医学院.中药大辞典(上册) [M]. 1997:1234.
    [7] 瞿发林,董文燊,刘 蓉,杨 婷,等.不同产地青风藤中青藤碱的含量比较[J].药物研究,2010,19(18):32.
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Analysis of volatile constituents in Caulis Sinomenii by GC-MS

doi: 10.3969/j.issn.1006-0111.2012.02.010
  • Department of Pharmacy, Eastern Hepatobilliary Hospital, Second Military Medical University, Shanghai 200438, China
  • Received Date: 2011-08-29
  • Rev Recd Date: 2011-12-28

Abstract: Objective To establish the determination method for chemical constituents of the volatile oil in Sinornenium actum(Thunb.)Rehd.et Wils by gas chromatography-mass spectrometry(GC-MS). Method The volatile oil was extracted from Sinornenium actum(Thunb.)Rehd.et Wils by steam distillation.The constituents of volatile oil were identified by GC-MS technology,which were identified through database index. Results The results showed that after comparing of the gained mass spectrum with the standard, 63 kinds of chemical constituents in all were identified, the major constituents were the fatty acids, sterols, alkenes and a few kind of aldehyde. The most contents were octadecylic acid and hexadecanoic acid, whose relative percentages were 33.78% and 23.23% respectively. Conclusion The experiment improved the basic components study on Caulis Sinomenii, which could provide more reference quality control of Caulis Sinomenii.

CHEN Jun, ZHOU Jin, HE Yun-xin, FENG Chun-hua, ZHANG Guo-qing. Analysis of volatile constituents in Caulis Sinomenii by GC-MS[J]. Journal of Pharmaceutical Practice and Service, 2012, 30(2): 115-117. doi: 10.3969/j.issn.1006-0111.2012.02.010
Citation: CHEN Jun, ZHOU Jin, HE Yun-xin, FENG Chun-hua, ZHANG Guo-qing. Analysis of volatile constituents in Caulis Sinomenii by GC-MS[J]. Journal of Pharmaceutical Practice and Service, 2012, 30(2): 115-117. doi: 10.3969/j.issn.1006-0111.2012.02.010
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